- Description
- Inquiry
CE 602 Discontinuous Rectification Educational Equipment Thermal Laboratory Equipment
Distillation is used to separate liquid mixtures made up of individual liquids that are soluble in one another. Rectification refers to distillation in a counterflow. Ethanol/water is recommended as the liquid mixture for the CE 602. The liquid mixture is added to the evaporator (bottom) tank. The mixed vapour produced moves upwards in the column. The mixed vapour contains a higher concentration of the component with the lower boiling point (ethanol). It leaves the top of the column and is condensed using a condenser and a phase separation tank. Part of the condensate is collected in a tank as product while the rest is fed back into the column. Here, on its way downwards, it undergoes further heating and material exchange with the rising mixed vapour. This exchange causes the vapour phase to become richer in ethanol and the liquid phase to become richer in water. The liquid phase moves to the bottom where it is collected.
A sieve tray column and a packed column are available. The packed column is filled with Raschig rings. The reflux ratio is adjusted using valves.
Relevant measured values are recorded by sensors and displayed digitally on the switch cabinet. The evaporator is adjusted using a PID controller.
A large, clear process schematic on the switch cabinet makes it easy to assign all the process variables.
Specification
discontinuous rectification with packed and sieve tray column
interchangeable columns
sieve tray column with 8 trays
packed column with Raschig rings
vacuum mode possible with water jet pump
electrically heated evaporator
tank for top product
condenser and phase separation tank for top product
all tanks made of DURAN glass and stainless steel
adjustment of reflux ratio using valves
8 temperature measuring points per column
Technical data
Columns: internal diameter: 50mm, height: 765mm
Water jet pump: final vacuum: approx. 200mbar
Tanks
top product: approx. 2000mL
phase separation: approx. 500mL
Evaporator
power output: 0…4kW
tank: approx. 10L
Heat transfer surface
top product condenser: approx. 0,04m2
Measuring ranges
temperature: 13x 0…150°C
reflux ratio: 0…100%
flow rate: 30…320L/h (cooling water)
differential pressure: 0…60mbar (column)
manometer: -1…0,6bar
400V, 50Hz, 3 phases
230V, 60Hz, 3 phases, 400V, 60Hz, 3 phases
UL/CSA optional
Dimensions and weight
LxWxH: 1300x750x2100mm
Weight: approx. 210kg
Required for operation
water connection: 500…1000L/h, drain
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Specification
[1] investigation of the pipe friction in laminar or turbulent flow on Hydraulic Bench
[2] transparent tank with overflow ensures constant water inlet pressure in the pipe section for experiments with laminar flow
[3] water supply via Base Module ( Hydraulic Bench) or via laboratory supply for experiments with turbulent flow
[4] flow rate adjustment via valves
[5] twin tube manometer for measurements in laminar flow
[6] dial-gauge manometer for measurements in turbulent flow
[7] flow rate determined by base module Hydraulic Bench
[8] water supply using base module ( Hydraulic Bench) or via laboratory supply
* Diameter of test pipe : 3.0mm ( Bore)
* Length of test pipe : 524mm
* Needle Valve included to regulate flow rate
length: 1000mm – Pipe section 1: acrylic 20×1.5mm – Pipe section 2: steel 1/2″ –
Smooth-bore pipes of various diameters Size – 6mm , 10mm, 17mm
Overall dimensions:
* Height : 1.05m form the ground level
* Width : 2.25m
* Depth : 0.43m
Test Pipe Diameters:
The Pipe network should have 90° Bends, 90° elbow,90°T, 45°elbow & Y.
Sudden enlargement
Sudden contraction
Ball Valve
Gate Valve
Globe valve
Inline strainer
Venturi made of clear acrylic
orifice palte made of clear acrylic
Pitot Static tube section made of clear acrylic
EXPERIMENTAL CAPABILITIES
Laminar to turbulent flow regimes in pipes
Energy losses in pipe fittings and bends
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Learning Objectives / Experiments
– flow measurement
– differential pressure measurement
– effect of flow and surface roughness
– effect of the flow velocity
– effect of changes in pipe direction
Specification
[1] investigation of the pressure loss at pipe elements with different changes in pipe direction and materials
[2] pipe elements are commercially standard components in heating and sanitary engineering
[3] clear panel mounted on a sturdy, movable frame
[4] simply selection of the measuring sections via hose connection with quick-release couplings
[5] flow can be adjusted via valves
[6] flow measurement using rotameter
[7] differential pressure measurement via differential pressure meter with display
Technical Data
Measuring sections: 2300mm
– pipe section 1: steel, diameter: 1/2″, 90° pipe angle
– pipe section 2: steel, diameter: 1/2″, 90° pipe bend
– pipe section 3: copper, diameter: 18x1mm,90° pipe angle
– pipe section 4: copper, diameter: 18x1mm,90° pipe bend
Differential pressure meter
Measuring ranges- flow rate: 150…1600L/h- differential pressure: -350mbar…350mbar
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investigation of the pressure losses of flow through pipes
– measurement of the pressure differential on different pipe sections
– influence of various pipe diameters
– influence of different materials and surface roughness
– effect of the flow velocity
– comparison between experiment and theory
Specification
[1] investigation of friction-induced pressure losses in flow through pipes
[2] pipe elements are commercially standard components in heating and sanitary engineering
[3] clear panel mounted on a sturdy, movable frame
[4] four measuring sections with different pipe crosssections and materials
[5] pipe sections can be selected via ball valves
[6] water connections made using quick-release couplings in the inflow and return
[7] flow can be adjusted via valves
[8] flow measurement using rotameter
[9] differential pressure measurement via differential pressure meter with display
Technical Data
Pipe sections measuring length: 1000mm
– pipe section 1: transparent plastic, diameter: 20×1,5mm
– pipe section 2: steel, diameter: 1/2″
– pipe section 3: copper, diameter: 18x1mm
– pipe section 4: copper, diameter: 15x1mm
Differential pressure meter
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– Variables affecting energy efficiency
* controller parameters
* refrigerant supercooling
– Interconnected operation of compressors
– Operation of a multicompressor controller
– Methods for returning oil in a multicompressor refrigeration system
– Representation of the thermodynamic cycle in the log p-h diagramSpecification
[1] Refrigeration system in multicompressor operation to investigate energy efficiency
[2] Refrigeration circuit with 3 compressors connected in parallel, condenser, thermostatic expansion valve and coaxial coil heat exchanger as evaporator
[3] Heat exchanger for refrigerant supercooling can be added via valves
[4] Glycol-water circuit includes pump and tank with heater serving as cooling load at the evaporator
[5] Multicompressor controller for the parallel operation of the compressors
[6] Separation of oil from the refrigerant on the delivery side and return to the intake side of the compressors
[7] Fan at the condenser with adjustable speed
[8] LabVIEW software for data acquisition via USB under Windows XP or Windows Vista
[9] Refrigerant R134a, CFC-free
Technical Data
3 compressors
– refrigeration capacity: each 1584W at -10°C/55°C
– power consumption: each 1156W at -10°C/55°C
Condenser with fan
– capacity: 4100W
– air flow: 1250m³/h
Coaxial coil heat exchanger capacity
– 4kW at ΔT=9K; 0,6m³/h glycol-water mixture
Glycol-water mixture pump
– max. flow rate: 5m³/h
– max. head: 6m
Heater power: 3kW
Tank
– glycol-water mixture: 23L
– refrigeration circuit receiver: 5,8L
Measuring ranges
– temperature: 4x 0…100°C, 4x -100°C…100°C
– pressure: 1x -1…9bar, 1x -1…24bar
– flow rate: 1x 1..25L/min
– compressor power: 0…4995W
Dimensions and Weight
l x w x h: 1800x700x1900mm
Weight: approx. 300kg
Connections
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Specification
[1] examination and comparison of various heat exchanger types
[2] five different types of heat exchangers included in the scope of delivery
[3] finned heat exchanger with fan
[4] operating mode (parallel flow or counter flow) selectable via valves
[5] flow rates adjustable via valves
[6] electromagnetic flow meter
[7] digital displays for temperature, pressure differences and flow rate
[8] hot & cold water benches available for
independent operation
[9] water/steam heat exchanger unit and electrical steam
Generator available for further experiments
[10] software for data acquisition via USB under Windows Vista or
Windows 7
Technical Data
Plate heat exchanger, 10 plates
– heat transfer surface area: approx. 0,26m²
– capacity: 15kW
Tubular heat exchanger
– heat transfer surface area: 0,1m²
– heat transfer surface area (coil): 0,17m²
Shell and tube heat exchanger
– capacity: 13kW
Finned cross-flow heat exchanger
– heat transfer surface area: approx. 2,8m²
– max. flow rate fan: 780m³/h
– max. pressure difference fan: 430Pa
Jacketed vessel with stirrer
– heat transfer surface area (vessel): 0,16m²
– heat transfer surface area (coil): 0,17m²
Measuring ranges
– differential pressure air: 0…10mbar
– differential pressure water: 0…1000mbar
– flow rate: 0…3m³/h
– temperature: 0…100°C
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– influence of pipe diameter, flow velocity, change in
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– determination of pump characteristics, system characteristics and the operating point
Specification
[1] investigation of the pressure losses at contractions, pipe angles, pipe bends, valves and fittings and pipe elements of different diameter
[2] pipe elements are commercially standard components in heating and sanitary engineering
[3] clear panel mounted on a sturdy, movable frame
[4] closed water circuit with pump and tank
[5] integrated bleed valve on manometer and in the pipe section
[6] flow measurement using rotameter
[7] measurement of the pressure distribution at
13 pressure measuring points, display with 13 tube manometers
Technical Data
Pump – 3 stages – max. flow rate: 4,5m³/h – max. head: 6m
Tank: approx. 5L
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